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Sodium Feredetate BP Grade Manufacturers, SDS MSDS Sheet

Sodium Feredetate: CAS Number: 15708-41-5, EINECS EC Number: 239-802-2, Molecular Formula: C10H12FeN2NaO8, Molecular Weight: 367.05 HS Code ---**

For MSDS Sheet Click
MSDS Sheet of Sodium Feredetate Manufacturers

Sodium Feredetate
BP & Commercial Pure Grade
Sodium Feredetate

Synonyms: Edathamil monosodium ferric salt; Ferric sodium EDTA; Iron monosodium EDTA; Iron sodium ethylenediaminetetraacetate; Monosodium ferric EDTA; Sodiumferric EDTA; Sodium iron EDTA; EDTA--Fe Na

Sodium feredetate or sodium ironedetate an un-ionised form containing iron in ferric form, which has been used as an iron fortificant of foods. The only advantage that has been shown is that in the presence of dietary inhibitors of iron absorption (like phytates), the relative bioavailability of iron in this preparation is higher (2-3 times) compared to that of ferrous sulphate.

Specifications of Sodium Feredetate Trihydrate Commercial Pure
Chemical Formula: C10H12FeN2NaO8.3H2O
Molecular Weight: 421.09 gms
Appearance: Light yellow coloured powder.
Identification: Confirm to Test
Solubility: Soluble in water.
pH (1% solution): 3.5 to 6.5
Assay (as Fe): 12.5% to 13.5%
Assay (as EDTA): 65.5% to 70.5%
NTA: N.M.T. 0.1%
Arsenic: N.M.T. 1 Ppm
Lead: N.M.T. 1 Ppm

Sodium Feredetate BP Grade
C10H21N2O8FeNa,H2Oıı385.1ıı15708-41-5 (anhydrous)

DEFINITION
Sodium Feredetate is iron(III) sodium ethylenediaminetetra-acetate monohydrate. It contains not less than 98.0% and not more than 102.0% of C10H12O8N2FeNa, calculated with reference to the dried substance.

CHARACTERISTICS
A yellow or yellowish brown, crystalline powder; hygroscopic.

IDENTIFICATION
A. The infrared absorption spectrum is concordant with the reference spectrum of sodium feredetate.
B. Ignite 0.5 g and allow to cool. Dissolve the residue in 2 ml of hydrochloric acid , add sufficient water to produce 20 ml and filter. The filtrate yields reaction C characteristic of iron salts. Dilute 1 volume of the filtrate to 10 volumes with water; the solution yields reaction B characteristic of iron salts.
C. Dissolve 2 g in 30 ml of water, slowly add 6.5 ml of a 20% w/v solution of potassium hydroxide, shake and filter the resulting suspension. Evaporate 8 ml of the filtrate to dryness, ignite and dissolve the residue in 4 ml of water. The solution yields reaction B characteristic of sodium salts.

TESTS
Acidity: pH of a 1% w/v solution, 4.0 to 6.5.
Free iron: Not more than 500 ppm when determined by the following method.
Dissolve 0.2 g in sufficient water to produce 20 ml and filter. Label three tubes A, B and C. Place 5 ml of the filtrate into each of tubes A and B and 4 ml of water and 1 ml of an iron standard solution prepared in the following manner in tube C. For the iron standard solution dilute 25 volumes of a 0.1726% w/v solution of ammonium iron(III) sulphate in 0.05M sulphuric acid to 200 volumes with water (25 ppm of Fe(III)). Add 1 ml of a 1.0% w/v solution of disodium catechol-3,5-disulphonate into each of tubes A and C and 1 ml of water to tube B. Measure the absorbance of solution A at 670 nm using solution B in the reference cell and of solution C using water in the reference cell. The absorbance of solution A is not greater than that of solution C.
Heavy metals: 1 g complies with limit test D for heavy metals 20 ppm.
Free sodium edetate: To 4 ml of a 1.0% w/v solution add 2 ml of ferric iron standard solution (50 ppm) and 1 ml of a 1.0% w/v solution of disodium catechol-3,5-disulphonate and mix. Prepare a standard in the same manner using 4 ml of a 0.010% w/v solution of disodium edetate in place of the solution of the substance being examined. Measure the absorbance of the solutions at 670 nm using water in the reference cell. The absorbance of the solution of the substance being examined is not less than that of the standard solution (1%).
Sulphates: Dissolve 2 g in 40 ml of water, add 5 ml of a 20% w/v solution of sodium hydroxide and sufficient water to produce 50 ml, shake and filter. Evaporate 6.2 ml of this solution to drynessand ignite until no trace of carbon remains. Cool and dissolve the residue in 10 ml of distilled water. Neutralise the solution with 2M hydrochloric acid using litmus paper as external indicator and add 2 ml in excess. Boil the solution, cool, dilute to 15 ml with distilled water and filter. The filtrate complies with the limit test for sulphates 600 ppm.
Loss on drying: When dried over silica gel at 120° at a pressure not exceeding 2 kPa for 5 hours, loses 4.0 to 13.5% of its weight. Use 1 g.
ASSAY: Dissolve 1 g in 40 ml of water in an iodine flask, add 20 ml of hydrochloric acid and 3 g of potassium iodide, close the flask and allow to stand for 5 minutes. Titrate the liberated iodine with 0.1M sodium thiosulphate VS using starch mucilage as indicator. Repeat the procedure without the substance being examined. The difference between the titrations represents the amount of sodium thiosulphate required. Each ml of 0.1M sodium thiosulphate VS is equivalent to 36.71 mg of C10H12O8N2FeNa.

For Original Monographs of IP Indian Pharmacopoeia BP British Pharmacopoeia USP US Pharmacopoeia FCC Food Grade product, please check with the respective web-pages or books.

Manufacturers:

MUBY CHEMICALS
Ambernath Mumbai, Ankleshwar Gujarat, India
TEL: (OFFICE) 91-22-23770100, 23726950
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e-mail: info@mubychem.com

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Last 18 May, 2017

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Sodium Feredetate Anhydrous SDS, Safety Data Sheet

1. Product Identification

Synonyms: Sodium Feredetate.
CAS No.: 15708-41-5
EINECS: EC Number: 239-802-2
Molecular Weight: 367.05
Chemical Formula: C10H12FeN2NaO8
Recommended usage: Industrial Manufacturing.
Suppliers: As per letterhead above.

2. Hazards Identification

GHS, Globally Harmonized System Classification in accordance with 29 CFR910
Classification according to Regulation (EC) No 1272/2008

Generally described as non-hazardous as per GHS, however, we will prefer to add the following warning.

Skin corrosion/irritation Category 2 (H315)
Serious eye damage/eye irritation Category 2A (H319)
Specific target organ toxicity, single exposure; Respiratory tract irritation Category 3 (H335)

Labeling according GHS & Regulation (EC) No 1272/2008

GHS Label Elements
Irritant
Irritant

Signal Word: Warning

Hazard Statements:
H315 : Causes skin irritation.
H319: Causes serious eye irritation.
H335: May cause respiratory irritation.

Precautionary Statements
P260: Do not breathe dust/fume/gas/mist/vapors/spray.
P264: Wash thoroughly after handling.
P280-Wear protective gloves/protective clothing/eye protection/face protection.
P314: Get Medical advice/attention if you feel unwell.
P362: Take off contaminated clothing and wash before reuse.
P302+P352 - IF ON SKIN: Wash with plenty of soap and water.
P303+P361+P353 - IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower.
P304+340: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305+P351+P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P332+P313: If skin irritation occurs: Get medical advice/attention.
P337+P313 If eye irritation persists: Get medical advice/ attention.
P402: Store in a dry place.

Classification according to EU Directives 67/548/EEC or 1999/45/EC:
Hazard symbols:
Xi Irritant
R-phrase(s):
R36/37/38 Irritating to eyes, respiratory system and skin.
S-phrase(s):
S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36 Wear suitable protective clothing.
OSHA Hazards: Irritant

3. Composition/Information on Ingredients

Ingredient: Sodium Feredetate anhydrous
CAS No.: 15708-41-5
EINECS: EC Number: 239-802-2

4. First Aid Measures

Always seek medical attention after first aid measures are provided.

Inhalation: Remove to fresh air. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get medical attention.
Ingestion: Never give anything by mouth to an unconscious person. Get medical attention.
Skin Contact: Wipe off excess material from skin then immediately flush skin with plenty of water for at least 15 minutes. Remove contaminated clothing and shoes. Get medical attention. Wash clothing before reuse. Thoroughly clean shoes before reuse.
Eye Contact: Immediately flush eyes with plenty of water for at least 15 minutes, lifting lower and upper eyelids occasionally. Get medical attention immediately.
Note to Physician: Symptomatic and supportive treatment is recommended.

5. Fire Fighting Measures

Flammability of the Product: Non-flammable.
Flash Points: Not applicable.
Products of Combustion: Carbon oxides, nitrogen oxides (NOx), Sodium oxides, Iron oxides.
Fire: Sodium Feredetate is not flammable.
Explosion: Not likely.
Fire Extinguishing Media: Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide.
Special Information: In the event of a fire, wear full protective clothing and NIOSH-approved self-contained breathing apparatus with full face piece operated in the pressure demand or other positive pressure mode. At high temperatures or when moistened under fire conditions, it may produce toxic or irritating fumes.

6. Accidental Release Measures

Small Spill: Avoid dust formation. Avoid breathing dust. Ensure adequate ventilation. Use appropriate tools to put the spilled solid in a convenient waste disposal container. Finish cleaning by spreading water on the contaminated surface and dispose of according to local and regional authority requirements.
Large Spill: Do not let the product enter drains. Use a shovel to put the material into a convenient waste disposal container. Finish cleaning by spreading water on the contaminated surface and allow evacuating through the sanitary system.

7. Handling and Storage

Do not breathe dust. Wear suitable protective clothing. In case of insufficient ventilation, wear suitable respiratory equipment.
Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Wash hands thoroughly after handling. Provide appropriate exhaust ventilation at places where dust is formed. If you feel unwell, seek medical attention.
Keep Sodium Feredetate Anhydrous in a tightly closed container, stored in a cool, dry, ventilated area. Protect against physical damage or contact with water and strong oxidizing agents.

8. Exposure Controls/Personal Protection

Airborne Exposure Limits: Not established.
Ventilation System: A system of local and/or general exhaust is recommended to keep employee exposures as low as possible. Local exhaust ventilation is generally preferred because it can control the emissions of the contaminant at its source, preventing dispersion of it into the general work area.
Personal Respirators (NIOSH Approved): For conditions of use where exposure to dust or mist is apparent and engineering controls are not feasible, a particulate respirator may be worn. For emergencies or instances where the exposure levels are not known, use a full-face positive-pressure, air-supplied respirator.
Skin Protection: Wear protective gloves and clean body-covering clothing.
Eye Protection: Use chemical safety goggles and/or full face shield where dusting or splashing of solutions is possible. Maintain eye wash fountain and quick-drench facilities in work area.
Other Control Measures: Maintain good housekeeping in work area. Dust deposits on floors and other surfaces may pick up moisture and cause the surfaces to become slippery and present safety hazards. Handle in accordance with good industrial hygiene and safety practice. Wash hands after handling.

9. Physical and Chemical Properties

Appearance: Sodium Feredetate Anhydrous is yellow powder or granules/flakes/lumps.
Odor: None.
Solubility: Soluble in water.
pH: 4.5.
Density: 1.78 gm/cc at 20C
Melting Point: ~80 °C
Molecular Weight: 367.05
Chemical Formula: C10H12FeN2NaO8
% Volatiles by volume @ 21C (70F): 0

10. Stability and Reactivity

Stability: Sodium Feredetate Anhydrous very delinquent in nature. It is stable under ordinary conditions of use and storage.
Hazardous Decomposition Products: Carbon oxides, nitrogen oxides (NOx), Sodium oxides, Iron oxides.
Hazardous Polymerization: Will not occur.
Incompatibilities: Strong Oxidizing agents.
Conditions to Avoid: Incompatibles. Avoid dusting.

11. Toxicological Information

Toxicity to Animals:
LD50 Oral - rat - 5,000 mg/kg
Carcinogenic Effects: Not a reported carcinogen by IARC NTP ACGIH OSHA.

12. Ecological Information

Toxicity to fish: LC50 - Pimephales promelas (fathead minnow) - 100 mg/l - 96 h
Toxicity to daphnia and other aquatic invertebrates: LC50 - Daphnia magna (Water flea) - 13 mg/l - 96 h
Environmental Fate: Not expected to be a short term hazard.

13. Disposal Considerations

Whatever cannot be saved for recovery or recycling should be managed in an appropriate and approved waste disposal facility. Processing, use or contamination of this product may change the waste management options. State and local disposal regulations may differ from federal disposal regulations. Dispose of container and unused contents in accordance with federal, state and local requirements. Small amounts of this material may be suitable for sanitary sewer or trash disposal.

14. Transport Information

DOT (USA)
Not Regulated.
IMDG
Not Regulated.
IATA
Not Regulated.
ADR/RID:
Not Regulated.

15. Regulatory Information

USA:
SARA 302
: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302.
SARA 313: This material does not contain any chemical components with known CAS numbers that exceed the threshold reporting levels established by SARA Title III, Section 313.
SARA 311/312 Hazards: No SARA Hazards

Canada: May cause sentisation by skin contact. Irritating to eyes, respiratory system and skin.

Section 16 - Additional Information

EINECS: EC Number: 239-802-2
H315 = Causes skin irritation.
H319 = Causes serious eye irritation.
H335 = May cause respiratory irritation.
Xi = Irritant
R36/37/38 = Irritating to eyes, respiratory system and skin.

Disclaimer:
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Our company provides this MSDS sheet in good faith but makes no representation as to its comprehensiveness or accuracy. This SDS sheet is intended only as a guide to the appropriate precautionary handling of the material by a properly trained person using this product. The above information has been compiled from various sources and has the possibility of discrepancy and being out-dated information. Individuals receiving the information must exercise their independent judgment and do further search in determining its appropriateness for a particular purpose. In no case shall our company be liable to loss or damages by the product user.
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