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Mubychem Group, established in 1976, is the pioneer manufacturer of Zinc Chloride, Ammonium Chloride, Calcium Chloride, Potassium Chloride, Sodium Acetate, Sodium Thiosulphate, Pharmaceutical, Fragrance & Flavor chemicals in India.  Mubychem Group has several manufacturing facilities spread across Gujarat and Maharashtra (Western India). 

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Sodium Acetate IP Technical & Pure Grade

 

Sodium Acetate USP Specifications

Sodium Acetate

C2H3NaO2·3H2O 136.08

 

Assay—  Sodium Acetate contains three molecules of water of hydration, or is anhydrous. It contains not less than 99.0 percent and not more than 101.0 percent of C2H3NaO2, calculated on the dried basis.

Packaging and storage— Preserve in tight containers.

Labeling— Label it to indicate whether it is the trihydrate or is anhydrous. Where Sodium Acetate is intended for use in hem dialysis, it is so labeled.

Identification— A solution responds to the test for Sodium and for Acetate.

pH: between 7.5 and 9.2, in a solution in carbon dioxide-free water containing the equivalent of 30 mg of anhydrous sodium acetate per mL.

Loss on drying— Dry at 120 to constant weight: the hydrous form loses between 38.0% and 41.0% of its weight, and the anhydrous form loses not more than 1.0% of its weight.

Insoluble matter— Dissolve the equivalent of 20 g of anhydrous sodium acetate in 150 mL of water, heat to boiling, and digest in a covered beaker on a steam bath for 1 hour. Filter through a tarred filtering crucible, wash thoroughly, and dry at 105 : the weight of the residue does not exceed 10 mg (0.05%).

Chloride— A portion equivalent to 1.0 g of anhydrous sodium acetate shows no more chloride than corresponds to 0.50 mL of 0.020 N hydrochloric acid (0.035%).

SulfateA portion equivalent to 10 g of anhydrous sodium acetate shows no more sulfate than corresponds to 0.50 mL of 0.020 N sulfuric acid (0.005%).

Calcium and magnesium— To 20 mL of a solution containing the equivalent of 10 mg of anhydrous sodium acetate per mL add 2 mL each of 6 N ammonium hydroxide, ammonium oxalate TS, and dibasic sodium phosphate TS: no turbidity is produced within 5 minutes.

Potassium— Dissolve the equivalent of 3 g of anhydrous sodium acetate in 5 mL of water, add 1N acetic acid drop wise until the solution is slightly acidic, and then add 5 drops of sodium cobalt nitrite TS: no precipitate is formed.

Aluminum (where it is labeled as intended for use in hem dialysis)— the limit is 0.2µ =g per g.

Heavy metals—the limit is 0.001%.

Organic volatile impurities: meets the requirements.


 

Sodium Acetate Trihydrate BP Specifications

C2H3NaO2,3H2Oıı

Action and use

Used in solutions for dialysis; excipient.

DEFINITION

Sodium ethanoate trihydrate.

Content

99.0 per cent to 101.0 per cent (dried substance).

CHARACTERS

Appearance

Colourless crystals.

Solubility

Very soluble in water, soluble in ethanol (96 per cent).

IDENTIFICATION

ıA. 1 ml of solution S (see Tests) gives reaction (b) of acetates.

ıB. 1 ml of solution S gives reaction (a) of sodium.

ıC. Loss on drying (As shown in the Relevant Test).

TESTS

Solution S

Dissolve 10.0 g in carbon dioxide-free water prepared from distilled water R and dilute to 100 ml 100 ml with the same solvent.

Appearance of solution

Solution S is clear and colourless.

pH

7.5 to 9.0.

Dilute 5 ml of solution S to 10 ml with carbon dioxide-free water.

Reducing substances

Dissolve 5.0 g in 50 ml of water, then add 5 ml of dilute sulphuric acid and 0.5 ml of

0.002 M potassium permanganate. The pink colour persists for at least 1 h. Prepare a blank in the same manner but without the substance to be examined.

Chlorides

Maximum 200 ppm.

Sulphates

Maximum 200 ppm.

Aluminium

Maximum 0.2 ppm, if intended for use in the manufacture of dialysis solutions.

Arsenic

Maximum 2 ppm, determined on 0.5 g.

Calcium and magnesium

Maximum 50 ppm, calculated as Ca.

Heavy metals

Maximum 10 ppm.

Iron

Maximum 10 ppm, determined on 10 ml of solution S.

Loss on drying

39.0 per cent to 40.5 per cent, determined on 1.000 g by drying in an oven at 130 °C.


 

Sodium Acetate as per US Food Chemical Codex

C2H3NaO2 Formula wt, anhydrous 82.03

C2H3NaO2·3H2O Formula wt, trihydrate 136.08

 

DESCRIPTION

Sodium Acetate occurs as colorless, transparent crystals or as a granular, crystalline or white powder. The anhydrous form is hygroscopic; the trihydrate effloresces in warm, dry air. One gram of the anhydrous form dissolves in about 2 mL of water; 1 g of the trihydrate dissolves in about 0.8 mL of water and in about 19 mL of alcohol.

Function Buffer.

 

REQUIREMENTS

Identification A 1:20 aqueous solution gives positive tests for Sodium and for Acetate,

Assay Not less than 99.0% and not more than 101.0% of C2H3NaO2 after drying.

Alkalinity Anhydrous: Not more than 0.2%; Trihydrate: Not more than 0.05%.

Lead Not more than 2 mg/kg.

Loss on Drying Anhydrous: Not more than 1.0%; Trihydrate: Between 36.0% and 41.0%.

Potassium Compounds Passes test.


 

Sodium Acetate as per ACS specifications
American Chemical Society Reagent Grade
Sodium Acetate, Anhydrous

CH3COONa                                                  
Formula Wt 82.03

CAS Number 127-09-3

 

REQUIREMENTS

Assay                                                               99.0% C2H3O2Na

pH of a 5% solution                                          7.0-9.2 at 25C


MAXIMUM ALLOWABLE

Insoluble matter                                                0.01%

Loss on drying at 120C                                 1.0%

Chloride (Cl)                                                    0.002%

Phosphate (PO4)                                              0.001%

Sulfate (SO4)                                                    0.003%

Calcium (Ca)                                                    0.005%

Magnesium (Mg)                                              0.002%

Heavy metals (as Pb)                                        0.001%

Iron (Fe)                                                          0.001%


 

Sodium Acetate Trihydrate as per ACS specifications
American Chemical Society Reagent Grade

NaC2H3O2 . 3H2O                               
Formula Wt 136.08

CAS Number 6131-90-4

 

REQUIREMENTS

Assay                                                               99.0-101% NaC2H3O2 . 3H2O

pH of a 5% solution                                          7.5-9.2 at 25C

Substances reducing permanganate                   Passes test


MAXIMUM ALLOWABLE

Insoluble matter                                                0.005%

Chloride (Cl)                                                    0.001%

Phosphate (PO4)                                              5 ppm

Sulfate (SO4)                                                    0.002%

Heavy metals (as Pb)                                        5 ppm

Iron (Fe)                                                          5 ppm

Calcium (Ca)                                                    0.005%

Magnesium (Mg)                                              0.002%

Potassium (K)                                                  0.005%

 

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Sodium Acetate manufacturer Sodium Acetate at:
MUBY CHEMICALS

S-8, SARIFA MANSION, 2ND FLANK ROAD, CHINCHBUNDER, MUMBAI 400009, INDIA.

TEL: (OFFICE) 91-22-23770100, 23726950, 23774610, 23723564. FAX: 91-22-23728264.

 e-mail: info@mubychem.com

Cell Call to Anmol: +91-9821870100 or Ambrish: +91-9821570100

Sodium Acetate Manufacturer

 

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Old Spice: Manufacturing since more than Three Decades:

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