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Calcium Undecylenate USP n Pure Grade Manufacturers, SDS GHS MSDS Sheet
Calcium Undecylenate: CAS Number: 1322-14-1, EINECS EC Number: 215-331-8, Molecular Formula: C22H38CaO4, Molecular Weight: 406.61 HS Code ---**
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SDS MSDS Sheet of Calcium Undecylenate Manufacturers
Pure n USP Grade
Calcium Undecylenate is the calcium salt of undecylenic acid, an 11 carbon mono-unsaturated fatty acid with broad-spectrum antifungal activity. Undecylenic acid inhibits the morphogenesis of Candida albicans to its invasive fungal form and inhibits the conversion of unicellular yeast to their hyphal form. Calcium Undecylenate is also known as Calcium diundec-10-enoate; 10-Undecenoic acid, calcium salt; 10-Undecenoic acid, calcium salt (2:1). It is a very economical anti-fungal agent and is used as an active ingredient in many topical over the counter anti-fungal preparations, both powders and ointments. It is an extremely effective, well-tolerated, broad-spectrum anti fungal. It is reported to be specially effective for athletes' foot and similar infections.
Calcium Undecylenate USP Grade
C22H38O4Ca -- 406.61
10-Undecenoic acid, calcium (2+) salt.
Calcium Undecylenate contains not less than 98.0 percent and not more than 102.0 percent of C22H38O4Ca (calcium undecylenate), calculated on the dried basis.
Packaging and storage: Preserve in well-closed containers.
A: A filtered solution (1 in 20) in 3 N hydrochloric acid responds to the tests for Calcium.
B: Transfer 40 mL of water and 10 g of calcium undecylenate to a 250-mL separator. Cautiously and slowly add 10 mL of hydrochloric acid, while swirling. Insert the stopper, and shake. [NOTE—The separator will become quite warm, and pressure must be carefully and frequently relieved through the stopcock. If a curdy, white material remains after 5 minutes of shaking, add additional hydrochloric acid, 1 mL at a time, and shake until a clear oily phase is formed.] Allow the phases to separate, drain, and discard the bottom aqueous layer. Drain and discard the middle oily layer, if present. Filter the top layer of undecylenic acid through a pledget of cotton into a 10-mL graduated cylinder, noting the volume obtained. Transfer the filtrate to a 250-mL flask, and add an equal volume of aniline. Reflux for 1 hour, swirling the flask occasionally. Allow to cool, and pour 60 mL of alcohol through the condenser into the flask. Remove the flask from the condenser, add 1 g of charcoal, and stir. Filter the slurry into a 250-mL beaker. Add water drop-wise until a few crystals form or the solution becomes slightly cloudy. [NOTE—If too much water is added, an oil will form. Add alcohol dropwise until the oil dissolves.] Allow the mixture to stand or refrigerate until crystals are formed. Collect the crystals on a filter paper inserted in a 45-mm porous glass filter funnel. Wash the crystals with 75 mL of 25% alcohol: the crystals have a clean, white, glossy appearance. If not, re-crystallize by dissolving the crystals in about 50 mL of alcohol. Add about 1 g of charcoal, stir, filter into a 150-mL beaker, and continue as directed above, beginning with “Add water dropwise.” Dry the crystals in vacuum at 50C for 2 hours: the crystals so obtained melt between 66 and 67.5. [NOTE—If the melting point is low, additional drying or recrystallization may be necessary.]
Loss on drying: Dry it at 105 for 2 hours: it loses between 2.0% and 5.7% of its weight.Assay: Boil 40.0 mL of 0.1 N hydrochloric acid with about 600 mg of Calcium Undecylenate, accurately weighed, for 10 minutes, or until the undecylenic acid layer is clear, adding water, as necessary, to maintain the original volume. Transfer the mixture, with the aid of water, to a 500-mL separator. Dilute with water to about 75 mL, and extract with two 100-mL portions of solvent hexane. Wash the combined extracts with water until the last washing is neutral to litmus, add the washings to the original water layer. Cool, add 3 drops of methyl orange, and titrate the excess hydrochloric acid with 0.1 N sodium hydroxide. Perform a blank determination. Each mL of 0.1 N sodium hydroxide is equivalent to 20.33 mg of C22H38O4Ca.
Particle size, Method: Test in accordance with this procedure, except to use not more than 25 g, and except that a single No. 100 sieve is used and is to be shaken for not less than 30 minutes or until sifting is practically complete: not less than 99.0% of it passes through a No. 100 sieve.
Limit of free undecylenic acid: Transfer 10 g of Calcium Undecylenate, accurately weighed, to a 400-mL beaker, add 250 mL of solvent hexane, and mix for 2 hours using a magnetic stirrer. Filter into a 500-mL flask, evaporate with the aid of a current of air to about 20 mL, and add 100 mL of neutralized alcohol. Add 3 drops of phenolphthalein TS, and titrate with 0.1 N sodium hydroxide. Each mL of 0.1 N sodium hydroxide is equivalent to 18.43 mg of C11H20O2: not more than 0.1% is found.
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Last : 11 April, 2017
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Calcium Undecylenate SDS MSDS Sheet, Material Safety Data Sheet
Section 1: Chemical Product and Identification
Product Name: 10-Undecenoic acid, calcium (2+) salt
EINECS EC-No.: 215-331-8
Chemical Formula: C22H38CaO4
Intended Use: Laboratory and Industrial Manufacturing.
SUPPLIER: As per letterhead.
Section 2: Hazards Identification
GHS, Globally Harmonized System Classification in accordance with 29 CFR 1910
Classification according to Regulation (EC) No 1272/2008
Not a hazardous substance or mixture according to Regulation (EC) No. 1272/2008.
This substance is not classified as dangerous according to Directive 67/548/EEC.
Labeling according to GHS & Regulation (EC) No 1272/2008
GHS Label Elements
Signal Word: None
Not considered hazardous by the OSHA Hazard Communication Standard (29 CFR 1910.1200)
Hazards not otherwise classified (HNOC):
May causes mild skin irritation.
May Causes mild eye irritation.
P261: Avoid breathing dust/fume/gas/mist/vapors/spray.
P302+P352 - IF ON SKIN: Wash with plenty of soap and water.
P303+P361+P353 - IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower.
P304 + P340 - IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338 - IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P337+313: If eye irritation persists get medical advice/attention.
Section 3: Composition and Information on Ingredients
Composition: Calcium Undecylenate
EINECS EC-No.: 215-331-8
% by Weight: 100
Section 4: First Aid Measures
Always seek medical attention after first aid measures are provided.
Eye Contact: In case of contact, immediately flush eyes with plenty of water for at least 15 minutes. Get medical attention.
Skin Contact: In case of contact, immediately flush skin with plenty of water. Cover the irritated skin with an emollient. Thoroughly clean shoes and clothes before reuse. Get medical attention.
Inhalation: If Calcium Undecylenate is inhaled, remove to fresh air. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get medical attention.
Ingestion: Do NOT induce vomiting unless directed to do so by medical personnel. Never give anything by mouth to an unconscious person. If large quantities of this material are swallowed, call a physician immediately.
Section 5: Fire and Explosion Data
Flammability of the Product: Calcium Undecylenate may be combustible at high temperature.
Auto-Ignition Temperature: Not available.
Products of Combustion: Some metallic oxides CO CO2 and fumes.
Fire Hazards in Presence of Various Substances: Slightly flammable in presence of heat. Non-flammable in presence of shocks.
Explosion Hazards in Presence of Various Substances: Slightly explosive in presence of open flames and sparks. Non-explosive in presence of shocks.
Fire Fighting Media and Instructions:
Small Fire: Use DRY chemical powder.
Large Fire: Use water spray, fog or foam. Avoid water jet.
Section 6: Accidental Release Measures
Small Spill: Avoid dust formation. Avoid breathing vapors, mist or gas. Use appropriate tools to put the spilled solid in a convenient waste disposal container. Finish cleaning by spreading water on the contaminated surface and dispose of according to legal authority requirements.
Large Spill: Use a shovel to put the material into a convenient waste disposal container. Finish cleaning by spreading water on the contaminated surface and allow drain.
Section 7: Handling and Storage
Precautions: Keep away from heat. Keep away from sources of ignition. Do not breathe dust.
Storage: Keep Calcium Undecylenate container tightly closed. Keep container in a cool, well-ventilated area.
Section 8: Exposure Controls/Personal Protection
Exposure Limits: Not established.
Engineering Controls: Use process enclosures, local exhaust ventilation, or other engineering controls to keep airborne levels below recommended exposure limits. If user operations generate dust, fume or mist, use ventilation to keep exposure to airborne contaminants below the exposure limit.
Personal Protection: Safety glasses. Lab coat. Dust respirator. Be sure to use an approved/certified respirator or equivalent. Gloves.
Exposure Limits: Not available.
Section 9: Physical and Chemical Properties
Physical state and appearance: Calcium Undecylenate is solid.
Odor: Not available.
Taste: Not available.
Chemical Formula: C22H38CaO4
pH (1% soln/water): Not available.
Melting Point: Not available.
Solubility: Not available.
Section 10: Stability and Reactivity Data
Stability: It is stable.
Conditions of Instability: Excessive heat, dust generation
Incompatibility with various substances: Oxidizing Agents, heat and sunlight.
Special Remarks on Reactivity: Decomposes on heating.
Hazardous decomposition products formed under fire conditions: Carbon oxides, Calcium oxide.
Polymerization: Will not occur.
Section 11: Toxicological Information
Toxicity to Animals: Not available.
Carcinogenicity: No component of this product present at levels greater than or equal to 0.1% is identified as probable or confirmed human carcinogen by IARC, ACGIH, OSHA and NTP.
Mutagenic Effects: Not available.
Teratogenic Effects: Not available.
Environmental Toxicity: Not available.
Section 12: Ecological Information
Ecotoxicity: Not available.
Products of Biodegradation: Possibly hazardous short term degradation products are not likely. However, long term degradation products may arise.
Toxicity of the Products of Biodegradation: The product itself and its products of degradation are not toxic.
Section 13: Disposal Considerations
Waste Disposal: Waste must be disposed of in accordance legal regulations.
Section 14: Transport Information
DOT (US): Not dangerous goods
ADR/RID: Not dangerous goods
TDG/IMDG: Not dangerous goods
IATA: Not dangerous goods
Section 15: Other Regulatory Information
HMIS (Perceived): Health Hazard: 1; Fire Hazard: 1; Reactivity: 0; Personal Protection: E
NFPA (Perceived): Health: 1; Flammability: 1; Reactivity: 0
Canada WHMIS: Not controlled under WHMIS (Canada).
EINECS EC-No.: 209-725-9
Section 16 - Additional Information
DISCLAIMER: The information and recommendations set forth herein (hereinafter "Information") are presented in good faith and believed correct as of the date hereof. It is compiled from various sources and it is not necessarily all inclusive nor fully adequate in every circumstance. In addition, these suggestions should not be confused with nor followed in violation of applicable laws, regulations, rules or insurance requirements applicable. This MSDS sheet is intended only as a guide to the appropriate precautionary handling of the material by a properly trained person using this product. Individuals receiving the information must exercise their independent judgment in determining its appropriateness for a particular purpose.