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Magnesium Pidolate & Pure Grade Manufacturers, SDS GHS MSDS Sheet

Magnesium Pidolate: CAS Number: 62003-27-4, EINECS EC Number: 263-365-7, Molecular Formula: C10H12N2O6Mg, Molecular Weight: 280.5 HS Code ---**

For MSDS Sheet Click
SDS MSDS Sheet of Magnesium Pidolate Manufacturers

Magnesium Pidolate
Pure BP & Pure Grade
Magnesium Pidolate

Magnesium pidolate, the magnesium salt of pidolic acid (pyroglutamic acid), is a mineral supplement.

Magnesium Pidolate BP Grade
Ph Eur
C10H12N2O6Mg -- 280.5 -- 62003-27-4

DEFINITION
Magnesium bis[(2S)-5-oxopyrrolidine-2-carboxylate].
Content: 8.49 per cent to 8.84 per cent of Mg (Ar = 24.31) (anhydrous substance).

CHARACTERS
Appearance: Amorphous, white or almost white powder, hygroscopic.
Solubility: Very soluble in water, soluble in methanol, practically insoluble in methylene chloride.

IDENTIFICATION
A. Thin-layer chromatography.
Test solution: Dissolve 60 mg in 2 ml of water and dilute to 10 ml with methanol.
Reference solution: Dissolve 55 mg of pidolic acid CRS in 2 ml of water and dilute to 10 ml with methanol.
Plate:TLC silica gel plate.
Mobile phase: methanol, glacial acetic acid, methylene chloride (15:20:65 V/V/V).
Application:1 μl.
Development: Over 2/3 of the plate.
Drying: At 100-105C for 15 min.
Detection: Spray with concentrated sodium hypochlorite solution. Allow to stand for 10 min and spray abundantly with glacial acetic acid. Allow to stand again for 10 min and dry the plate at 100-105C for 2 min. Spray with potassium iodide and starch solution until spots appear.
Results: The principal spot in the chromatogram obtained with the test solution is similar in position, colour and size to the principal spot in the chromatogram obtained with the reference solution. The chromatogram obtained with the test solution may show 2 faint secondary spots.
B. To 0.15 ml of solution S (see Tests) add 1.8 ml of water. The solution gives the reaction of magnesium.

TESTS
Solution S: Dissolve 5.00 g in carbon dioxide-free water prepared from distilled water and dilute to 50.0 ml with the same solvent.
Appearance of solution: Solution S is clear and not more intensely coloured than reference solution.
pH: 5.5 to 7.0 for solution S.
Specific optical rotation: - 23.3 to - 26.5 (anhydrous substance), determined on solution S.
Related substances:
Liquid chromatography.
Test solution: Dissolve 0.500 g of the substance to be examined in the mobile phase and dilute to 100.0 ml with the mobile phase.
Reference solution (a): Dilute 1.0 ml of the test solution to 100.0 ml with the mobile phase.
Reference solution (b): Dissolve 50.0 mg pidolate impurity B CRS in the mobile phase and dilute to 100.0 ml with the mobile phase. Dilute 5.0 ml of the solution to 50.0 ml with the mobile phase.
Reference solution (c): Dilute 10.0 ml of reference solution (b) to 100.0 ml with the mobile phase.
Reference solution (d): Dilute 1.0 ml of nitrate standard solution (100 ppm NO3) to 100.0 ml with the mobile phase.
Reference solution (e): Dilute 6.0 ml of reference solution (a) to 10.0 ml with reference solution (b).
Column:
size: = 0.25 m, Ø = 4.6 mm;
stationary phase: octadecylsilyl silica gel for chromatography (5 μm).
Mobile phase: Dissolve 1.56 g of sodium dihydrogen phosphate R in 1000 ml of water R and adjust to pH 2.5 with a 10 per cent V/V solution of phosphoric acid R.
Flow rate: 1.5 ml/min.
Detection: Spectrophotometer at 210 nm.
Injection: 10 μl loop injector; inject the test solution and reference solutions (b), (c), (d) and (e).
Run time: 4 times the retention time of pidolic acid.
Retention times: Pidolic acid = about 4.5 min; impurity B = about 7.5 min.
System suitability: Reference solution (e):resolution: minimum 10 between the peaks due to pidolic acid and to impurity B.
Limits:
impurity B: not more than the area of the principal peak in the chromatogram obtained with reference solution (b) (1.0 per cent);
total of other impurities: not more than half of the area of the principal peak in the chromatogram obtained with reference solution (b) (0.5 per cent);
disregard limit: not more than 0.5 times the area of the principal peak in the chromatogram obtained with reference solution (c) (0.05 per cent); disregard any peak corresponding to the nitrate ion (NO3–).

Impurity A
Thin-layer chromatography.
Test solution: Dissolve 0.250 g of the substance to be examined in 4 ml of water and dilute to 50.0 ml with methanol.
Reference solution (a): Dissolve 60.0 mg of glutamic acid R in 50 ml of water R and dilute to 100.0 ml with methanol. Dilute 1.0 ml of the solution to 20.0 ml with methanol.
Reference solution (b): Dissolve 10 mg of glutamic acid and 10 mg of aspartic acid in water and dilute to 25 ml with the same solvent. Dilute 1 ml of the solution to 10 ml with water.
Plate:TLC silica gel plate R.
Mobile phase: glacial acetic acid, water, butanol (20:20:60 V/V/V).
Application: 5 μl.
Development: Over 2/3 of the plate.
Drying: In air.
Detection: Spray with ninhydrin solution and heat at 100-105C for 15 min.
System suitability: The test is not valid unless the chromatogram obtained with reference solution (b) shows 2 clearly separated spots.
Limit:
impurity A: any spot corresponding to impurity A in the chromatogram obtained with the test solution is not more intense that the spot in the chromatogram obtained with reference solution (a) (0.6 per cent).
Chlorides: Maximum 500 ppm.
Nitrates: Examine the chromatogram obtained with the test solution in the test for related substances.
Limit:
nitrates: not more than the area of the principal peak in the chromatogram obtained with reference solution (d) (200 ppm).
Sulphates: Maximum 0.1 per cent.
Arsenic: Maximum 2 ppm.
Iron: Maximum 200 ppm.
Heavy metals: Maximum 20 ppm.
Water: Maximum 8.0 per cent, determined on 0.200 g.

ASSAY
Dissolve 0.300 g in 50 ml of water. Carry out the complexometric titration of magnesium.
1 ml of 0.1 M sodium edetate is equivalent to 2.431 mg of Mg.

IMPURITIES
A. glutamic acid,
B. (2S)-2-[[[(2S)-5-oxopyrrolidin-2-yl]carbonyl]amino]pentanedioic acid.

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Manufacturers:

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Last 14 August, 2017

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Magnesium Pidolate SDS GHS, MSDS Sheet, Material Safety Data Sheet

Section 1: Chemical Product and Company Identification

Product Name: Magnesium Pidolate.
Synonym:
Magnesium salt of pidolic acid, Pyroglutamic acid, Magnesium (S)-2-pyrrolidone-5-carboxylate, Magnesium 5-oxo-L-proline.
CAS Number: 62003-27-4
EINECS EC Code: 263-365-7
Molecular Formula: C10H12N2O6Mg
Molecular Weight: 280.5
Recommended usage: Industrial Manufacturing.
Suppliers: As per letterhead.

Section 2: Hazards Identification

GHS, Globally Harmonized System Classification in accordance with 29 CFR 1910
Hazard Class and Category Code(s), Regulation (EC) No 1272/2008 (CLP)

Not a hazardous substance or mixture according to Regulation (EC) No. 1272/2008.
This substance is not classified as dangerous according to Directive 67/548/EEC.

Labeling Regulation as per GHS & EC 1272/2008 (CLP) & GHS

GHS Label Elements
NONE

Signal Word: None

Hazards not otherwise classified (HNOC):
May causes mild skin irritation.
May causes mild eye irritation.

Precautionary statements:
P261: Avoid breathing dust/fume/gas/mist/vapors/spray.
P262: Do not get in eyes, on skin, or on clothing.
P281: Use personal protective equipment as required.
P302+P352 - IF ON SKIN: Wash with plenty of soap and water.
P303+P361+P353 - IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower.
P304 + P340 - IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338 - IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P337+313: If eye irritation persists get medical advice/attention.

Section 3: Composition and Information on Ingredients

Product Name: Magnesium Pidolate.
CAS Number
: 62003-27-4
EINECS EC Code: 263-365-7
Percentage: >97%

Section 4: First Aid Measures

Always seek medical advice after the first aid treatment.

Skin: Rinse with water. Soap may be used. Seek Medical Aid.
Eyes: Wash eyes with plenty of water for at least 15 minutes, lifting lids occasionally. Seek Medical Aid.
Inhalation: Remove to fresh air. If not breathing, give artificial respiration. If breathing is difficult, give oxygen.
Ingestion: If swallowed, induce vomiting immediately after giving two glasses of water. Never give anything by mouth to an unconscious person.

Section 5: Fire and Explosion Data

Flammability of the Product: Non-flammable.
Products of Combustion: Carbon oxides, nitrogen oxides (NOx), Magnesium oxide.
Fire Fighting Media and Instructions: Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide. Wear self-contained breathing apparatus for firefighting if necessary.

Section 6: Accidental Release Measures

Small Spill: Use appropriate tools to put the spilled solid in a convenient waste disposal container. Finish cleaning by spreading water on the contaminated surface and dispose of according to legal requirements.
Large Spill: Do not inhale vapors, mist, or gas. Avoid dust formation. Use a shovel to put the material into a convenient waste disposal container. Finish cleaning by spreading water on the contaminated surface and allow to evacuate through the sanitary system. Be careful that the product is not present at a concentration level above TLV. Check TLV with local authorities.

Section 7: Handling and Storage

Precautions: Do not breath the dust. Keep away from incompatibles such as oxidizing agents, acids.
Storage: Keep container tightly closed. Keep container in a cool, well-ventilated area. Hygroscopic. Handle and store under inert gas.

Section 8: Exposure Controls/Personal Protection

Engineering Controls: Use process enclosures, local exhaust ventilation, or other engineering controls to keep airborne levels below recommended exposure limits. If user operations generate dust, fume or mist, use ventilation to keep exposure to airborne contaminants below the exposure limit.
Personal Protection: Safety glasses. Lab coat. Dust respirator. Be sure to use an approved/certified respirator or equivalent Gloves.
Personal Protection in Case of a Large Spill: Splash goggles. Full suit. Dust respirator. Boots. Gloves. A self contained breathing apparatus should be used to avoid inhalation of the product. Suggested protective clothing might not be sufficient; consult a specialist BEFORE handling this product.

Section 9: Physical and Chemical Properties
Physical state and appearance: Solid white crystals or powder.
Odor: NA.
Specific Gravity: NA.
pH (10% soln/water): about 5.5 to 7.
Melting point/freezing point: NA.
Solubility: Soluble in water.
Molecular Formula: C10H12N2O6Mg
Molecular Weight: 280.5

Section 10: Stability and Reactivity Data

Stability: It is stable in closed containers under recommended storage & handling.
Conditions of instability: Incompatible materials, Moisture
Incompatibility with various substances: Avoid high temperatures, sparks, open flames and moisture. Avoid contact with strong oxidizing agents.
Polymerization: Will not occur.

Section 11: Toxicological Information

No toxicological data available for this product.
The toxicological properties of this substance have not been fully investigated.
Carcinogenic Effects: Not a reported carcinogen by IARC, NTP, ACGIH, OSHA.

Section 12: Ecological Information

Toxicity to fish: Not available.
BOD5 and COD: Not available.
Products of Biodegradation: The product itself and its products of degradation are not toxic. The product is expected to be biodegradable.

Section 13: Disposal Considerations

Waste Disposal: Waste must be disposed of in accordance with federal, state and local environmental control regulations.

Section 14: Transport Information

DOT (US): Not dangerous goods
IMDG: Not dangerous goods
IATA: Not dangerous goods
ADR/RID: Not dangerous goods

Section 15: Other Regulatory Information

USA Regulations:
SARA 302: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302.
SARA 313: This material does not contain any chemical components with known CAS numbers that exceed the threshold (De Minimis) reporting levels established by SARA Title III, Section 313.
SARA 311/312 Hazards: No SARA Hazards
California Prop. 65 Components: This product does not contain any chemicals known to State of California to cause cancer, birth defects, or any other reproductive harm.

Canada:
WHMIS Hazard Class: Not controlled.

EINECS EC Code: 263-365-7

Section 16 - Additional Information

DISCLAIMER: The information and recommendations set forth herein (hereinafter "Information") are presented in good faith and believed correct as of the date hereof. It is compiled from various sources and it is not necessarily all inclusive nor fully adequate in every circumstance. In addition, these suggestions should not be confused with nor followed in violation of applicable laws, regulations, rules or insurance requirements applicable. This MSDS sheet is intended only as a guide to the appropriate precautionary handling of the material by a properly trained person using this product. Individuals receiving the information must exercise their independent judgment in determining its appropriateness for a particular purpose.